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I typed up my official report for the University of Toledo's chemical library.

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The quality control results matched!

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I calculated MOMIPP's theoretical percent composition of carbon, hydrogen, nitrogen, and oxygen.

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These results came back positive with few impurities.

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I did a more specific NMR test with a fancier machine.

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We got results from the quality control testing.

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I did thin light chromatography again. This is what the diluted sample I tested looked like.

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We analyzed further decided that the NMR results were good enough to send off for quality control testing.

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We started to analyze the results for this time around

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Back to the NMR!

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I calculated the final percent yield.

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I filtered my final product.

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And.......it took me a while to get this part right.

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I preformed the second half of the synthesis  under reflux (constant supply of heat energy barely below the boiling point.)

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I measured out my materials for the second part of the synthesis.

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I tested my sample with thin light chromatography.

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Back to stoichiometry!

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I calculated my percent yield.

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We analyzed the results and they looked good.

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I did a test called nuclear magnetic resonance (NMR) to determine the composition of my product at the atomic level. I wasn't allowed to bring my phone into the room so here's a picture from Google of what it looked like.

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After letting the final product of the first reaction dry, this is what I got.

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I started the reaction while being careful to not expose it to oxygen.

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Lots of measuring out materials!

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I did plenty of stoichiometry to determine how much of each material I needed.

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Dr. Erhardt and his graduate student sat down with me and explained how MOMIPP is made.